Browsing by Subject "WINES"
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Item HPLC-UV and GC-MS characterization of the flavonol aglycons quercetin, kaempferol, and myricetin in tomato pastes and other tomato-based products(UNIV SILESIA, INST CHEMISTRY) Tokusoglu, Ö; Ünal, MK; Yildirim, ZThe amounts of three flavonoids, quercetin, kaempferol, and myricetin, in tomatoes (Solanum lycopersicum L.) and tomato-based products produced in Turkey has been determined by reversed phase high-performance liquid chromatography (RPHPLC) with UV detection. The HPLC profiles of five types of tomato, one commercial composite tomato juice, and three types of tomato paste, were obtained after acid hydrolysis and extraction. The presence of the flavonol aglycons was confirmed by gas chromatography with mass spectrometric detection (GC-MS). Tomatoes and tomato-based products contained primarily quercetin, kaempferol, and the minor flavonol myricetin. The total flavonol aglycon content of different varieties of tomato varied from 3.1 to 10.0 mg kg(-1) of fresh weight. Tomato juice and tomato salsa were rich in total flavonols, containing 19.8 mg L-1 and 10.5-13.2 mg kg(-1), respectively. The method enabled accurate and reproducible quantitative analysis of these flavonols in tomatoes and tomato-based products.Item ALTERATIONS ON PHENOLIC COMPOUNDS AND ANTIOXIDANT ACTIVITY DURING SOUR GRAPE JUICE CONCENTRATE PROCESSING(ESTACAO VITIVINICOLA NACIONAL) Guler, A; Tokusoglu, O; Artik, NThe alterations of phenolic compounds and antioxidant capacity of sour grape juice were investigated during the concentration process stages. Phenolics and antioxidant properties of the samples changed more at the vacuum evaporation stage than that of the other stages. After evaporation, the antioxidant capacity of the samples decreased approximately between 14.2 and 17.0 % for DPPH and ABTS methods, respectively. Besides, phenolic contents also decreased approximately as 14.8%. HPLC data on phenolics of sour grape juice during concentrate processing gave 12 polyphenols, including gallic acid, (+)-catechin, (-)-epigallocatechin, vanillic acid, (-)-epigallocatechin gallate, (-)-epicatechin, caftaric acid, caffeic acid and p-coumaric acid, which were determined as 1.05-1.83 mg/100 g, 5.40-7.83 mg/100 g, 6.35-9.21 mg/100 g, 3.01-5.18 mg/100 g, 0-1.95 mg/100 g, 2.33-3.54 mg/100 g, 12.40-37.60 mg/100 g, 1.44-2.26 mg/100 g and 0.27-0.44 mg/100 g, respectively. Ferulic, sinapic acids and quercetin were only detected at concentrate step of the sour grape juice processing and were found as 0.18 mg/100 g, 0.28 mg/100 g and 0.76 mg/100 g, respectively.