Properties of Aluminum Nano Composites Bearing Alumina Particles and Multiwall Carbon Nanotubes Manufactured by Mechanical Alloying and Microwave Sintering

Özer E.; Ayvaz M.; Übeyli M.; Sarpkaya İ.

Properties of Aluminum Nano Composites Bearing Alumina Particles and Multiwall Carbon Nanotubes Manufactured by Mechanical Alloying and Microwave Sintering

Date

2023

Authors

Publisher

Korean Institute of Metals and Materials

Abstract

Abstract: In this research, the effects of heat treatment and hybrid reinforcement ratio on the microstructural and mechanical properties of Al–4Cu nanocomposites containing MWCNT and nano Al2O3p were investigated. First of all, the hybrid reinforced Al–4Cu nanocomposites were manufactured with the aid of mechanical alloying and microwave sintering. And then, they were subjected to various heat treatments; annealing and artificial aging at 170, 180 and 200 °C individually. After that, the microstructural observations were made using X-ray diffraction, optical microscope and scanning electron microscopes (SEMs). The secondary electrons (SE), back scattered electrons (BSE), energy dispersive X-ray (EDX) and elemental mapping analyses of the specimens were carried out with the aid of SEMs. In addition, the nanoindentation tests were done to get the nanohardness and elastic modulus of composites. Finally, the composites were subjected to the compression test to clarify their compressive properties. The Al2Cu and Al4C3 precipitates were detected in the composite samples either annealed or peak-aged at 200 °C, while the intermetallic compound, Al7Cu2Fe, precipitated only in the aged samples. A significant increment in the nanohardness of composites was obtained with increasing reinforcement content. Moreover, the elastic modulus of annealed and peak-aged composites, reinforced with 15% hybrid reinforcement in volume, increased by 59% and 57%, respectively compared to the unreinforced alloy. Furthermore, the use of hybrid reinforcement in the alloy matrix allowed an improvement of compressive yield strength at the expense of compressive strain. Graphical Abstract: [Figure not available: see fulltext.]. © 2022, The Author(s) under exclusive licence to The Korean Institute of Metals and Materials.